in water incomplete saturation of an aq. ClI solution with NaOH;; isolation of iodate from formed NaCl by fractional crystallization; recrystallization of the precipitate from water; drying at 25 °C;;
in water incomplete saturation of an aq. ClI solution with Na2CO3;; isolation of iodate from formed NaCl by fractional crystallization; recrystallization of the precipitate from water; drying at 25 °C;;
in neat (no solvent) mild warming of equivalent amounts of ICl and CH3COONa;; product mixture;;
参考文献
Schuetzenberger, P.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1861 , vol. 52, p. 135 - 135
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Gmelin Handbook: I: MVol.2, 102, page 467 - 469
