in chloroform
addn. of soln. of ICl in CHCl3 to soln. of Co-compd. in CHCl3 (darkness, room temp., N2 atmosphere, 45 min); concn., pouring into ether, filtration, washing (ether), chromy. (silica gel, CH2Cl2:MeOH:pyridine 90:9:1 vol/vol);
参考文献
Gupta, B. D.; Kumar, Manjo
Inorganica Chimica Acta, 1991 , vol. 181, p. 73 - 80
hydrogen in gas
Irradiation (UV/VIS); at low ICl-pressure down to 20mm Hg pressure and H2-pressure of 1atm.;;
参考文献
Iredale, T.; Mellor, D. P.
Journal of the American Chemical Society, 1931 , vol. 53, p. 2802 - 2802
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Mellor, D. P.; Iredale, T.
Nature (London, United Kingdom), 1930 , vol. 127, p. 93 - 93
in acetic acid
equivalent amounts of educts, 0°C, closed vessel;;
参考文献
Cornog, J.; Horrobin, H. W.; Karges, R. A.
Journal of the American Chemical Society, 1938 , vol. 60, p. 429 - 432
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Gmelin Handbook: Pb: MVol.C2, 180, page 725 - 727
