L-2-((三氟甲基磺酰基)氧基)丙酸乙酯合成路线 （共 12 条）
反应条件
1: phenylacetonitrile; rac-2-(Trifluormethylsulfonyloxy)propionsaeure-ethylester With trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=130°C; Inert atmosphereMicrowave irradiationSealed tube;
2: acrylic acid With triethylamine in acetonitrile
T=150°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Jouanno, Laurie-Anne; Di Mascio, Vincent; Tognetti, Vincent; Joubert, Laurent; Sabot, Cyrille; Renard, Pierre-Yves
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1303 - 1319
反应条件
trimethylsilyl trifluoromethanesulfonate
T=120°C; 0.05 h; Inert atmosphereMicrowave irradiation;
参考文献
Jouanno, Laurie-Anne; Sabot, Cyrille; Renard, Pierre-Yves
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8549 - 8555
