4-氯-2-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)苯酚合成路线 （共 3 条）
反应条件
hydrogen; palladium on activated carbon in ethanol
P=750.075 Torr; 0.5 h; Product distribution / selectivity;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2006/21759 A1, 2006 ;
Location in patent: Page/Page column 32 ;
WO 2006/021759 A1
反应条件
1: boron tribromide / dichloromethane / 0.25 h / 0 °C / |Inert atmosphere
2: diethyl ether / 20 °C / |Inert atmosphere
View Scheme
参考文献
Friedman, Adam A.; Panteleev, Jane; Tsoung, Jennifer; Huynh, Vaizanne; Lautens, Mark
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9755 - 9758
反应条件
in diethyl ether
T=20°C; Inert atmosphere;
参考文献
Friedman, Adam A.; Panteleev, Jane; Tsoung, Jennifer; Huynh, Vaizanne; Lautens, Mark
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9755 - 9758
