反应条件
1: O2; azobis(isobutyronitrile) / acetonitrile / 0.5 h / 0 °C / Irradiation 2: Ph3P / acetonitrile; CH2Cl2 / 0 - 20 °C 3: 95 percent / 2,6-lutidine / CH2Cl2 4: 85 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 0 °C 5: 40 percent / trifluoroacetic anhydride; morpholine / acetonitrile 6: 20 percent / KHMDS / tetrahydrofuran / 2 h / -10 - 25 °C 7: 45 percent / FeCl2*4H2O / acetonitrile; H2O / 20 °C View Scheme
参考文献
O'Neill, Paul M.; Stocks, Paul A.; Pugh, Matthew D.; Araujo, Nuna C.; Korshin, Edward E.; Bickley, Jamie F.; Ward, Stephen A.; Bray, Patrick G.; Pasini, Erica; Davies, Jill; Verissimo, Edite; Bachi, Mario D.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 32 p. 4193 - 4197
