反应条件
1: Ph3P / acetonitrile; CH2Cl2 / 0 - 20 °C 2: 95 percent / 2,6-lutidine / CH2Cl2 3: 85 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 0 °C 4: 40 percent / trifluoroacetic anhydride; morpholine / acetonitrile 5: 20 percent / KHMDS / tetrahydrofuran / 2 h / -10 - 25 °C 6: 45 percent / FeCl2*4H2O / acetonitrile; H2O / 20 °C View Scheme
参考文献
O'Neill, Paul M.; Stocks, Paul A.; Pugh, Matthew D.; Araujo, Nuna C.; Korshin, Edward E.; Bickley, Jamie F.; Ward, Stephen A.; Bray, Patrick G.; Pasini, Erica; Davies, Jill; Verissimo, Edite; Bachi, Mario D.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 32 p. 4193 - 4197
