2-苄氧羰基氨基-1-乙醇合成路线 （共 31 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
SANKYO COMPANY, LIMITED
Patent: US2004/14962 A1, 2004 ;
Location in patent: Page/Page column 137 ;
反应条件
sodium hydrogencarbonate; ethanolamine in water T=20°C; 3 h;
参考文献
Pfizer Inc.
Patent: US6657063 B1, 2003 ;
Location in patent: Page column 94-95 ;
反应条件
sodium hydrogencarbonate in water; ethyl acetate
参考文献
Pfizer Products Inc.
Patent: EP994105 A2, 2000 ;
反应条件
TEA in tetrahydrofuran 5 h;
参考文献
Hara, Toshiaki; Durell, Stewart R.; Myers, Michael C.; Appella, Daniel H.
Journal of the American Chemical Society, 2006 , vol. 128, # 6 p. 1995 - 2004
反应条件
potassium carbonate in tetrahydrofuran T=20°C;
参考文献
Barcelo, Gerard; Senet, Jean-Pierre; Sennyey, Gerard; Bensoam, Jean; Loffet, Albert
Synthesis, 1986 , # 8 p. 627 - 632
反应条件
triethylamine in dichloromethane T=25°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 10 p. 3518 - 3534
反应条件
1: With triethylamine; isobutyl chloroformate in tetrahydrofuran 2: With sodium tetrahydroborate in water
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 7 p. 1975 - 1980
反应条件
methanol; sodium tetrahydroborate T=0°C; 0.333333 h; Yield given;
参考文献
Synthesis, , p. 299 - 301
反应条件
1: 1.)isobutyl chloroformate, N-methylmorpholine; 2.)triethylamine / 1.) THF, -15 deg C, 5 min; 2.) THF, -15 deg C, 1h 2: t-butyl thiol / tetrahydrofuran / Ambient temperature; Irradiation View Scheme
参考文献
Tetrahedron, , vol. 44, # 17 p. 5479 - 5486
反应条件
1: 94 percent / pyridine / CH2Cl2 / 5 h / Ambient temperature 2: 74 percent / aq. K2CO3 / tetrahydrofuran / 20 °C View Scheme
参考文献
Synthesis, , # 8 p. 627 - 632
