2-苄氧羰基氨基-1-乙醇合成路线 （共 31 条）
反应条件
Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1298 - 1299
反应条件
1: Et3N / CH2Cl2 / 1.) 0 deg C, 30 min, 2.) RT, 30 min 2: dimethylformamide / 3 h / 60 °C View Scheme
参考文献
Constantinou-Kokotou, Violetta; Kokotos, George
Organic Preparations and Procedures International, 1994 , vol. 26, # 5 p. 599 - 602
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; triphenylphosphine in tetrahydrofuran T=20°C; 2: With methylamine in tetrahydrofuran; ethanol T=20°C; 1 h; Further stages.;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 18, # 9 p. 2865 - 2870
反应条件
1: 88 percent / triethylamine / CH2Cl2 / 1.) 0 deg C, 30 min, 2.) RT, 30 min 2: 93 percent / sodium azide / hexamethylphosphoric acid triamide / 6 h / 55 °C 3: sodium borohydride / 10percent palladium on charcoal / H2O; methanol / Ambient temperature View Scheme
参考文献
Park, Jin-Hun; Oh, Chang-Hyun
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 2854 - 2860
反应条件
in dichloromethane T=25°C; 0.5 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5152 - 5155
反应条件
Erwaermen des Reaktionsprodukts;
参考文献
Ben-Ishai
Journal of the American Chemical Society, 1956 , vol. 78, p. 4962,4964
反应条件
tert.-butylhydroperoxide; Caldariomyces fumago chloroperoxidase in aq. acetate buffer T=20 - 23°C; pH=5; 30 h; Enzymatic reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 84, p. 144 - 151
反应条件
jones' reagent in acetone T=0°C; 3 h;
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: 95 percent / Jones' reagent / acetone / 3 h / 0 °C 2: 63 percent / DCC / CH2Cl2 / 10 h / Ambient temperature 3: Jones' reagent View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran; methanol P=760 Torr; 3 h; Ambient temperature;
参考文献
Yasuma, Tsuneo; Oi, Satoru; Choh, Nobuo; Nomura, Toshiyuki; Furuyama, Naoki; Nishimura, Atsushi; Fujisawa, Yukio; Sohda, Takashi
Journal of Medicinal Chemistry, 1998 , vol. 41, # 22 p. 4301 - 4308
