1,4-二苯基-3,4-二氢异喹啉合成路线 （共 8 条）
反应条件
1: in ethylene glycol dimethyl ether; diethyl ether; cyclohexane
T=-78 - 0°C;
2: With water in ethylene glycol dimethyl ether; diethyl ether; cyclohexane
参考文献
Kobayashi, Kazuhiro; Shiokawa, Taiyo; Omote, Hiroki; Hashimoto, Kenichi; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 7 p. 1126 - 1132
反应条件
tin(IV) chloride in chloroform
100 h;
参考文献
Nagubandi, Sreeramulu; Fodor, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1457 - 1463
反应条件
phosphorus pentoxide; toluene
参考文献
Krabbe
Chemische Berichte, 1936 , vol. 69, p. 1569,1571
反应条件
1: 95 percent / 15percent sodium hydroxide / H2O / 1 h / 0 °C
2: 92.3 percent / phosphorus pentachloride / benzene / 1.5 h
3: 95 percent / stannic chloride / CHCl3 / 100 h
View Scheme
参考文献
Nagubandi, Sreeramulu; Fodor, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1457 - 1463
反应条件
1: 95 percent / 15percent sodium hydroxide / H2O / 1 h / 0 °C
2: 92.3 percent / phosphorus pentachloride / benzene / 1.5 h
3: 95 percent / stannic chloride / CHCl3 / 100 h
View Scheme
参考文献
Nagubandi, Sreeramulu; Fodor, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1457 - 1463
反应条件
1.1: n-butyllithium / 1,2-dimethoxy-ethane; hexane / 0.25 h / 0 °C
1.2: 89 percent / 1,2-dimethoxy-ethane; hexane / 0.5 h
2.1: 1,2-dimethoxy-ethane; cyclohexane; diethyl ether / -78 - 0 °C
2.2: 69 percent / H2O / 1,2-dimethoxy-ethane; cyclohexane; diethyl ether
View Scheme
参考文献
Kobayashi, Kazuhiro; Shiokawa, Taiyo; Omote, Hiroki; Hashimoto, Kenichi; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 7 p. 1126 - 1132
参考文献
Krabbe
Chemische Berichte, 1936 , vol. 69, p. 1569,1571
参考文献
Dey; Ramanathan
Proceedings of the National Institute of Sciences of India, 1943 , vol. 9, p. 193,222
