in not given Cl3Si(OC2H5), Si(OC2H5)4 and CH3MgCl; hydrolysis;;
参考文献
Rathousky, J.; Chvalovsky, V.; Bazant, V.
Chemicke Listy, 1953 , vol. 47, p. 1387 - 1393
C. A., 1955 , p. 161
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Gmelin Handbook: Si: MVol.C, 107, page 296 - 298
in ethanol nitrate salt was dissolved and mixed with soln. of silicate in 1:1 mol. ratio, soln. was stirred at 40°C until gel was formed, xerogel was obtained by drying gel 24 h at 60°C, ground, heated to 500°C 1 h, then to 1300°C 24 h; XRD;
参考文献
Journal of the American Ceramic Society, , vol. 94, # 5 p. 1568 - 1574