反应条件
glycerine in ethanol mixt. of TiCl4, glycerine, ethanol, and tetraethoxysilane stirred vigorously at 25°C for 24 h; diluted with EtOH, atomized in N2 flow at 450°C; calcined at 450°C for 2 h; stirred at 30°C in HF/H2O/EtOH soln. for 40 h; solvents evapd. at 80°C;
参考文献
Zhu, Jian; Zhang, Dieqing; Bian, Zhenfeng; Li, Guisheng; Huo, Yuning; Lu, Yunfeng; Li, Hexing
Chemical Communications, 2009 , # 36 p. 5394 - 5396