反应条件
1: 1.) N-chlorosuccinimide, 2.) Et3N / 1.) CH2Cl2, room temperature, 30 min, 2.) -78 deg C, 2 h; room temperature, 1.5 h
2: 60 percent / pyridine, P2S5 / CH2Cl2 / 2.5 h
View Scheme
参考文献
Cutting, Ian; Parsons, Philip J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 21 p. 1209 - 1210