反应条件
lithium aluminium tetrahydride; n-butyllithium 1) THF, -78 deg C, 1 h, 2) THF, -78 deg C -> -5 deg C, 30 min, 3) THF, -5 deg C -> room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Jang, Won Bum; Shin, Won Suk; Hong, Jong Eun; Lee, Shi Yong; Oh, Dong Young
Synthetic Communications, 1997 , vol. 27, # 19 p. 3333 - 3339