1: With potassium carbonate Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling; 2: With Oxonereg; 12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
oxygen; chromium(II) acetate in ethyl acetate T=30°C; 2 h; different concentration of catalyst, diff. temperature, dependence of yield on time; Product distribution;
参考文献
Sandler; Khcheyan; Kharenko; Ryabukhin; Bobylev
Journal of applied chemistry of the USSR, 1984 , vol. 57, # 6 pt 2 p. 1244 - 1247
