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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丁烯酮
合成路线
（共 1452 条）
100-52-7
苯甲醛
+
78-94-4
丁烯酮
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
1: benzaldehyde With sodium cyanide in N,N-dimethyl-formamide T=35°C; Stetter reaction; 0.416667 h; 2: methyl vinyl ketone in N,N-dimethyl-formamide T=35°C; Stetter reaction; 2.33333 h;
参考文献
Ryzhkov; Andreev; Belov; Kurkin; Yurovskaya
Chemistry of Heterocyclic Compounds, 2011 , vol. 47, # 2 p. 182 - 193
5908-41-8
+
78-94-4
丁烯酮
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; isopropyl alcohol in tetrahydrofuran T=70°C; Sila-Stetter reaction;
参考文献
Mattson, Anita E.; Bharadwaj, Ashwin R.; Zuhl, Andrea M.; Scheidt, Karl A.
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5715 - 5724
32085-88-4
3,5-二氟苯甲醛
+
78-94-4
丁烯酮
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine in ethanol T=90°C; 1.5 h;
参考文献
MERMERIAN, Ara; Peng, Bo; Hudson, Colleen; Kim, Charles; Moore, Joel; Rohde, Jason; Sprott, Kevin; Graul, Regina; Nakai, Takashi; Jia, James; Bartolini, Wilmin
Patent: US2011/150834 A1, 2011 ;
Location in patent: Page/Page column 60-61 ;
78-94-4
丁烯酮
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran T=50°C; 2 h;
参考文献
Shirakawa; Yamamoto; Nakao; Tsuchimoto; Hiyama
Chemical Communications, 2001 , # 19 p. 1926 - 1927
201230-82-2
+
78-94-4
丁烯酮
+
108-90-7
氯苯
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
1: chlorobenzene With chloro-trimethyl-silane; zinc in tetrahydrofuran T=40°C; 4 h; 2: carbon monoxide; methyl vinyl ketone With tetrakis(triphenylphosphine) palladium(0); chloro-trimethyl-silane; lithium chloride in tetrahydrofuran T=30°C; P=760 Torr; 0.583333 h;
参考文献
Yuguchi, Motoki; Tokuda, Masao; Orito, Kazuhiko
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 908 - 914
622-42-4
+
78-94-4
丁烯酮
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
1: With potassium carbonate in water T=20°C; Michael addition; 3 h; 2: With dihydrogen peroxide; potassium carbonate in water T=20°C; Nef reaction;
参考文献
Ballini, Roberto; Barboni, Luciano; Giarlo, Guido
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9173 - 9176
201230-82-2
+
960-16-7
+
78-94-4
丁烯酮
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=80°C; P=30002.4 Torr; 18 h;
参考文献
Chochois, Helene; Sauthier, Mathieu; Maerten, Eddy; Castanet, Yves; Mortreux, Andre
Tetrahedron, 2006 , vol. 62, # 50 p. 11740 - 11746
201230-82-2
+
78-94-4
丁烯酮
+
98-80-6
→
反应条件
119-61-9
+
2550-26-7
+
583-05-1
1-苯基-1,4-戊二酮
反应条件
triphenylphosphine; rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate in methanol T=80°C; P=15001.2 Torr; 18 h;
参考文献
Tetrahedron, , vol. 62, # 50 p. 11740 - 11746
78-94-4
丁烯酮
+
591-51-5
→
反应条件
583-05-1
1-苯基-1,4-戊二酮
反应条件
1: phenyllithium; Mo(CO)6 in diethyl ether T=-60°C; Addition; 2: With boron trifluoride diethyl etherate in diethyl ether T=-60°C; Substitution; 0.25 h; 3: methyl vinyl ketone in diethyl ether T=-60 - 20°C; Addition; Further stages.;
参考文献
Barluenga, Jose; Rodriguez, Felix; Fananas, Francisco J.
Chemistry - A European Journal, 2000 , vol. 6, # 11 p. 1930 - 1937
5908-41-8
+
78-94-4
丁烯酮
→
反应条件
134-81-6
+
583-05-1
1-苯基-1,4-戊二酮
反应条件
n-Bu4N+CN- in tetrahydrofuran T=-78°C; 1 h;
参考文献
degl'Innocenti, Alessandro; Ricci, Alfredo; Mordini, Alessandro; Reginato, Gianna; Colotta, Vittoria
Gazzetta Chimica Italiana, 1987 , vol. 117, # 11 p. 645 - 648
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