N-[(苄氧基)羰基]甘氨酰-L-酪氨酸合成路线 (共 13 条)
反应条件
methanol; palladium Hydrogenation;
参考文献
Goldschmidt,S.; Rosculet,G.
Chemische Berichte, 1960 , vol. 93, p. 2387 - 2394
反应条件
orange flavedo peptide amidase; ammonium hydrogen carbonate in water; acetonitrile T=40°C; 72 h;
参考文献
Cerovsky, Vaclav; Kula, Maria-Regina
Angewandte Chemie - International Edition, 1998 , vol. 37, # 13-14 p. 1885 - 1887
反应条件
triethylamine in various solvent(s)
T=15°C; 10 h; pH=8; Yields of byproduct given;
参考文献
Kouge; Koizumi; Okai; Kato
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 7 p. 2409 - 2418
参考文献
Bergmann; Fruton
Journal of Biological Chemistry, 1937 , vol. 118, p. 405,414
反应条件
1: 75 percent / DEPBT; TEA / dimethylformamide / 20 °C
2: NaOH
View Scheme
参考文献
Xie; Tian; Ye
Synthetic Communications, 2000 , vol. 30, # 23 p. 4233 - 4240
反应条件
1: 75 percent / DEPBT; TEA / dimethylformamide / 20 °C
2: NaOH
View Scheme
参考文献
Xie; Tian; Ye
Synthetic Communications, 2000 , vol. 30, # 23 p. 4233 - 4240
反应条件
1: 81 percent / Et3N / acetonitrile / 1 h / 5 °C
2: 64 percent / Et3N / various solvent(s) / 10 h / 15 °C / pH=8
View Scheme
参考文献
Kouge; Koizumi; Okai; Kato
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 7 p. 2409 - 2418
反应条件
water
T=30°C; Peptidamidase aus dem Flavedo von Orangen; Yield given;
参考文献
Steinke, Doerte; Kula, Maria-Regina
Angewandte Chemie, 1990 , vol. 102, # 10 p. 1204 - 1206
反应条件
1: (i) PCl3, Py, (ii) /BRN= 4725904/
2: aq. NaOH / acetone
View Scheme
参考文献
Goldschmidt,S.; Rosculet,G.
Chemische Berichte, 1960 , vol. 93, p. 2387 - 2394
反应条件
1: ethyl acetate
2: aq. NaOH solution
View Scheme
参考文献
Bergmann; Fruton
Journal of Biological Chemistry, 1937 , vol. 118, p. 405,414