反应条件
1: 4-chlorobenzaldehyde With n-butyllithium; di-(2-methoxyethyl)amine in tetrahydrofuran; hexane
T=-20°C; 0.75 h; Inert atmosphere;
2: With n-butyllithium in tetrahydrofuran; hexane
T=-20 - 0°C; 2.16667 h; Inert atmosphere;
3: N,N-dimethyl-formamide Further stages;
参考文献
Kessler, Simon N.; Wegner, Hermann A.
Organic Letters, 2012 , vol. 14, # 13 p. 3268 - 3271