反应条件
1: 99 percent / imidazole; DMAP / CH2Cl2 / 3 h / 20 °C 2: 72 percent / oxone; aq. Na2EDTA; CF3COCH3 / NaHCO3 / acetonitrile / 0 °C 3: 74 percent / n-BuLi; CuCN; BF3*Et2O / diethyl ether; hexane / 2 h / -78 °C 4: OsO4; NaIO4 / ethanol; H2O / 24 h / 20 °C 5: 167 mg / NaBH4 / ethanol; H2O / 1 h / 20 °C 6: 99 percent / aq. HCl / dioxane / 1 h / Heating View Scheme
参考文献
Ouchi, Hidekazu; Mihara, Yukiko; Watanabe, Hitomi; Takahata, Hiroki
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7053 - 7056
