1-(4-氯苯基)-2,2,3,3,3-五氟-1-丙酮合成路线 (共 3 条)
反应条件
1: 4,4,4-trifluoro-1-(N-methoxy-N-methylamino)-1-phenyl-1-(trimethylsiloxyl)-2-butyne With tetrabutyl ammonium fluoride in tetrahydrofuran; diethyl ether T=-15°C; 0.166667 h; 2: pentafuoroethyl p-chlorophenyl ketone in tetrahydrofuran; diethyl ether T=20°C; 2 h;
参考文献
Jeong, In Howa; Jeon, Sung Lan; Kim, Bum Tae
Tetrahedron Letters, 2003 , vol. 44, # 38 p. 7213 - 7216
反应条件
diethyl ether; 4-chlorophenyl-magnesium bromide
参考文献
Kaluszyner; Cohen
Journal of Organic Chemistry, 1959 , vol. 24, p. 996
参考文献
Burton, Donald J.; Headley, James A.
Journal of Fluorine Chemistry, 1981 , vol. 18, p. 323 - 356