反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere<br />1.2: 4.75 h / -78 - -55 °C / |Inert atmosphere<br />2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -78 - 10 °C / |Inert atmosphere<br />2.2: 1.5 h / -5 °C / |Inert atmosphere<br /> <br />
参考文献
Van Rijssel, Erwin R.; Van Delft, Pieter; Van Marle, Daan V.; Bijvoets, Stefan M.; Lodder, Gerrit; Overkleeft, Herman S.; Van Der Marel, Gijsbert A.; Filippov, Dmitri V.; Code, Jeroen D.C. Journal of Organic Chemistry, 2015 , vol. 80, # 9 p. 4553 - 4565
