(2-氨基苯甲基)三苯基溴化膦合成路线 （共 27 条）
反应条件
1: With acetic acid in methanol
T=80°C; 0.166667 h; Microwave irradiationInert atmosphere;
2: With potassium tert-butylate in tetrahydrofuran
T=25°C; 1 h; Inert atmosphere;
参考文献
Kraus, George A.; Guo, Haitao
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5337 - 5341
反应条件
1: 76 percent / pyridine / CH2Cl2 / 0.5 h / Heating
2: 48 percent / t-BuOK / toluene / 0.5 h / Heating
View Scheme
参考文献
Eitel, Manfred; Pindur, Ulf
Synthesis, 1989 , # 5 p. 364 - 367
反应条件
1: NEt3 / CH2Cl2; toluene
2: 85 percent / MeONa / toluene / Heating
View Scheme
参考文献
Corre, M. Le; Hercouet, A.; Stanc, Y. Le; Baron, H. Le
Tetrahedron, 1985 , vol. 41, # 22 p. 5313 - 5320
反应条件
1: With acetic acid in methanol
T=80°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
2: With potassium tert-butylate in tetrahydrofuran
T=25°C; 1 h; Inert atmosphere;
参考文献
Kraus, George A.; Guo, Haitao
Organic Letters, 2008 , vol. 10, # 14 p. 3061 - 3063
反应条件
1: 71 percent / CH2Cl2 / 3 h
2: 70 percent / t-BuOK / toluene / 0.25 h / Heating
3: 82 percent / (CH3)3N*BH3, TFA / 0.25 h
View Scheme
参考文献
Coulton, Steven; Gilchrist, Thomas L.; Graham, Keith
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1193 - 1202
反应条件
1: With acetic acid in methanol
T=80°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
2: With potassium tert-butylate in tetrahydrofuran
T=25°C; 1 h; Inert atmosphere;
参考文献
Kraus, George A.; Guo, Haitao
Organic Letters, 2008 , vol. 10, # 14 p. 3061 - 3063
反应条件
1: 66 percent / CHCl3 / 12 h
2: 12 percent / KOtBu / toluene / 12 h / Heating
View Scheme
参考文献
Capuano, Lilly; Drescher, Stefan; Hammerer, Volker; Hanisch, Michael
Chemische Berichte, 1988 , vol. 121, p. 2259 - 2262
