N,N-二甲基咪唑-1-磺酰胺合成路线 (共 24 条)
反应条件
ammonium chloride in tetrahydrofuran; diethyl ether
参考文献
US6355665 B1, ;
US 6355665 B1
反应条件
n-butyllithium; triethylamine in tetrahydrofuran; hexane; ethyl acetate; benzene
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 2 p. 123 - 125
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 2 p. 123 - 125
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 2 p. 123 - 125
反应条件
methanesulfonic acid; phosphorous pentoxide T=70 - 90°C; 8 h;
参考文献
Kaboudin, Babak; Haghighat, Hamideh
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 951 - 955
反应条件
methanesulfonic acid; phosphorous pentoxide T=70 - 90°C; 12 h;
参考文献
Kaboudin, Babak; Haghighat, Hamideh
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 951 - 955
反应条件
1: N,N-Dimethyl-1H-imidazole-1-sulphonamide With n-butyllithium in tetrahydrofuran; hexane T=-78 - -35°C; 2: diphenyldisulfane in tetrahydrofuran; hexane T=-78 - 20°C; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 73, # 17 p. 6816 - 6823
反应条件
methanesulfonic acid; phosphorous pentoxide
T=70 - 90°C; 8 h;
参考文献
Kaboudin, Babak; Haghighat, Hamideh
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 951 - 955
反应条件
methanesulfonic acid; phosphorous pentoxide
T=70 - 90°C; 12 h;
参考文献
Kaboudin, Babak; Haghighat, Hamideh
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 951 - 955