N,N-二甲基咪唑-1-磺酰胺合成路线 （共 24 条）
反应条件
n-butyllithium
1.) DME, hexane, -5 deg C, 0.25 h, 2.) room temperature, 12 h; Yield given. Multistep reaction;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486
反应条件
n-butyllithium
1.) DME, hexane, -5 deg C, 0.25 h, 2.) -78 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486
反应条件
n-butyllithium
1.) DME, hexane, -5 deg C, 0.25 h, 2.) -78 deg C, 0.5 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in diethyl ether
T=20°C; 65 h; Inert atmosphere; regioselective reaction;
参考文献
Kallepalli, Venkata A.; Shi, Feng; Paul, Sulagna; Onyeozili, Edith N.; Maleczka Jr., Robert E.; Smith III, Milton R.
Journal of Organic Chemistry, 2009 , vol. 74, # 23 p. 9199 - 9201
