3-苯基-2-丙炔-1-胺合成路线 （共 15 条）
反应条件
in hexane 1.) ice bath, 2.) room temp., 21 h;
参考文献
Richey, Herman G.; Erickson, Wayne F.
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4349 - 4357
反应条件
in hexane 1.) ice bath, 2.) room temp., 21 h;
参考文献
Journal of Organic Chemistry, , vol. 48, # 23 p. 4349 - 4357
反应条件
copper(l) iodide; potassium carbonate; Tedicyp; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=80°C; 20 h;
参考文献
Lemhadri, Mhamed; Doucet, Henri; Santelli, Maurice
Synthesis, 2005 , # 8 art. no. Z22104SS, p. 1359 - 1367
反应条件
indium tribromide; triethylamine in diethyl ether
T=20°C; 1 h;
参考文献
Sakai, Norio; Hirasawa, Maki; Konakahara, Takeo
Tetrahedron Letters, 2003 , vol. 44, # 22 p. 4171 - 4174
反应条件
hydrogenchloride; sodium hydroxide; ammonia; benzaldehyde in water; toluene
参考文献
Sumitomo Chemical Company, Ltd.
Patent: US5756769 A1, 1998 ;
反应条件
hydrazine hydrate in methanol
2.5 h; Heating;
参考文献
Moody, Christopher J.; Rahimtoola, Kulsum F.; Porter, Barry; Ross, Barry C.
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2105 - 2114
反应条件
water in tetrahydrofuran
Reflux;
参考文献
Gorske, Benjamin C.; Mbofana, Curren T.; Miller, Scott J.
Organic Letters, 2009 , vol. 11, # 19 p. 4318 - 4321
反应条件
hydrogenchloride in tetrahydrofuran; 1,4-dioxane
T=20°C;
参考文献
Ishida, Tomonobu; Kobayashi, Ryo; Yamada, Tohru
Organic Letters, 2014 , vol. 16, # 9 p. 2430 - 2433
反应条件
phthalimide; di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine
1.) THF, RT, 3 d, 2.) THF, reflux; Yield given. Multistep reaction;
参考文献
Campi, Eva M.; Fallon, Gary D.; Jackson, W. Roy; Nilsson, Ylva
Australian Journal of Chemistry, 1992 , vol. 45, # 7 p. 1167 - 1178
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Knapp, Diana C.; Donofrio, Jennifer; Engels, Joachim W.
Bioconjugate Chemistry, 2010 , vol. 21, # 6 p. 1043 - 1055
