3-苯基-2-丙炔-1-胺合成路线 (共 15 条)
反应条件
1: 2) 30percent aq. NaOH / 1) THF, reflux
2: TosOH / methanol / Ambient temperature
View Scheme
参考文献
Morimoto, Toshiaki; Takahashi, Toshio; Sekiya, Minoru
Journal of the Chemical Society, Chemical Communications, 1984 , # 12 p. 794 - 795
反应条件
Sonogashira Cross-Coupling;
参考文献
Hase, Shun; Kayaki, Yoshihito; Ikariya, Takao
Organometallics, 2013 , vol. 32, # 19 p. 5285 - 5288
反应条件
hydrogen; triphenylphosphine; dirhodium tetraacetate
T=70°C; P=20685.9 Torr; 20 h;
参考文献
Campi, Eva M.; Jackson, W. Roy; Nilsson, Ylva
Tetrahedron Letters, 1991 , vol. 32, # 8 p. 1093 - 1094
反应条件
rhodium (II) acetate; hydrogen; triphenylphosphine in ethyl acetate
T=70°C; P=20685.9 Torr; 20 h;
参考文献
Campi, Eva M.; Fallon, Gary D.; Jackson, W. Roy; Nilsson, Ylva
Australian Journal of Chemistry, 1992 , vol. 45, # 7 p. 1167 - 1178
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in acetonitrile
T=50°C; 20 h; Inert atmosphere;
参考文献
Patil, Nitin T.; Raut, Vivek S.; Shinde, Valmik S.; Gayatri, Gaddamanugu; Sastry, G. Narahari
Chemistry - A European Journal, 2012 , vol. 18, # 18 p. 5530 - 5535