in methanol 15 h;

1: 25 percent / methanol / 1 h 2: 62 percent / 20 h View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '113916', constants.ctx, '0')">N-bromosuccinmide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1708400', constants.ctx, '0')">2,2'-azo-bisisobutyronitrile</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098295', constants.ctx, '0')">tetrachloromethane</a> <br />15&nbsp;h;&nbsp;&nbsp;HeatingIrradiation;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 1.) toluene, 16 h, reflux, 2.) ether<br />2: 13 percent / N-bromosuccinimide, bis(1-cyano-1-methylethyl)diazene / CCl₄ / 15 h / Heating; Irradiation<br /> <br /> &nbsp;