反应条件
1.1: LiBH4 / diethyl ether / 8 h / 0 °C
1.2: (COCl)2; Et3N; DMSO / CH2Cl2 / 6 h / -78 - 0 °C
1.3: 41 percent / CHI3; CrCl2 / tetrahydrofuran / 6 h / 23 °C
2.1: CuI; Pd(Ph3P)4; n-BuNH2 / benzene / 5 h / 23 °C
2.2: 61 percent / H2 / P-2 Ni / ethanol / 1.5 h / 760.05 Torr
3.1: 82 percent / n-Bu4NF / tetrahydrofuran / 8 h / 0 °C
4.1: 90 percent / NaOH / tetrahydrofuran; H2O / 7 h / 23 °C
View Scheme
参考文献
Jagadeesh; Reddy, L. Manmohan; Nasjletti, Alberto; Falck
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7111 - 7113
