2,3-二氢-1,4-苯并二氧杂环己-6-基甲酸酯合成路线 （共 3 条）
反应条件
potassium hydroxide in methanol T=20°C; 0.75 h;
参考文献
Hellberg, Jonas; Dahlstedt, Emma; Pelcman, Margit E.
Tetrahedron, 2004 , vol. 60, # 40 p. 8899 - 8912
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane; water
T=45°C; Bayer-Villiger oxidation; 17 h;
参考文献
Hellberg, Jonas; Dahlstedt, Emma; Pelcman, Margit E.
Tetrahedron, 2004 , vol. 60, # 40 p. 8899 - 8912
反应条件
1: 73 percent / KOH / methanol / 0.75 h / 20 °C
2: 71 percent / KH2PO4; NO(KSO3)2 / methanol; H2O / 1.42 h / Cooling
3: 75 percent / Na2S2O4 / H2O
View Scheme
参考文献
Hellberg, Jonas; Dahlstedt, Emma; Pelcman, Margit E.
Tetrahedron, 2004 , vol. 60, # 40 p. 8899 - 8912
