N-亚苄基-4-甲氧基苯胺合成路线 （共 139 条）
反应条件
DPDC in benzene
T=60°C; 5 h;
参考文献
Leardini, Rino; Nanni, Daniele; Pedulli, Gian Franco; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1591 - 1594
反应条件
DPDC in benzene
T=60°C; 5 h;
参考文献
Leardini, Rino; Nanni, Daniele; Pedulli, Gian Franco; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1591 - 1594
反应条件
1: 88 percent / t-BuOK / dimethylformamide / 12 h / Ambient temperature
2: 93 percent / H2SO4 / H2O / 2 h / 0 °C
View Scheme
参考文献
Van der Veen; Bari; Krishnan; Manhas; Bose
Journal of Organic Chemistry, 1989 , vol. 54, # 24 p. 5758 - 5762
反应条件
in tetrahydrofuran
T=70°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Shao, You-Dong; Wu, Xue-Song; Tian, Shi-Kai
European Journal of Organic Chemistry, 2012 , # 8 p. 1590 - 1596
反应条件
1.1: 69 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C
2.1: 94 percent / t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.67 h / 70 °C
3.1: t-BuLi; MeMgBr / tetrahydrofuran; pentane / -80 °C
3.2: 81 percent / tetrahydrofuran; pentane / -80 °C
4.1: 67 percent / H2 / Pd(OH)2/C / methanol / 1 h / 20 °C
5.1: 76 percent / CAN / H2O / 0.5 h / 0 °C
View Scheme
参考文献
Satoh, Tsuyoshi; Ozawa, Masaki; Takano, Koji; Chyouma, Tosio; Okawa, Akihiro
Tetrahedron, 2000 , vol. 56, # 26 p. 4415 - 4425
反应条件
1: 7 percent / various solvent(s) / 16 h / 160 - 165 °C
2: 0.7 g / potassium hydroxide / methanol; H2O / 5 h / Heating
3: 0.04 g / copper bronze / quinoline / 3 h / Heating
View Scheme
参考文献
Murphy, Shane T.; Taylor, Walter C.; Vadasz, Andrew
Australian Journal of Chemistry, 1982 , vol. 35, # 6 p. 1215 - 1225
反应条件
dicobalt octacarbonyl; benzene
T=230°C; P=147102 Torr;
参考文献
Murahashi et al.
Nippon Kagaku Zasshi, 1958 , vol. 79, p. 68,79
Chem.Abstr., 1960 , p. 5558
反应条件
antimony trichloride in acetonitrile
T=20°C; Diels-Alder reaction; 0.416667 h; stereoselective reaction;
参考文献
Varma, P. Prabhakara; Sherigara, Bailure S.; Mahadevan, Kittappa M.; Hulikal, Vijaykumar
Synthetic Communications, 2010 , vol. 40, # 15 p. 2220 - 2231
反应条件
antimony trichloride in acetonitrile
T=20°C; Diels-Alder reaction; 1.16667 h; stereoselective reaction;
参考文献
Varma, P. Prabhakara; Sherigara, Bailure S.; Mahadevan, Kittappa M.; Hulikal, Vijaykumar
Synthetic Communications, 2010 , vol. 40, # 15 p. 2220 - 2231
反应条件
ytterbium(III) triflate in acetonitrile
1.5 h; Ambient temperature;
参考文献
Makioka; Shindo; Taniguchi; Takaki; Fujiwara
Synthesis, 1995 , # 7 p. 801 - 804
