N-亚苄基-4-甲氧基苯胺合成路线 （共 139 条）
反应条件
ethanol bei Raumtemperatur;
参考文献
Bodforss
Justus Liebigs Annalen der Chemie, 1927 , vol. 455, p. 60
反应条件
in tetrahydrofuran T=70°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Shao, You-Dong; Wu, Xue-Song; Tian, Shi-Kai
European Journal of Organic Chemistry, 2012 , # 8 p. 1590 - 1596
反应条件
1: 1.) LDA / 2.) THF, -95 deg C to -78 deg C 2: cerium ammonium nitrate / tetrahydrofuran 3: 98 percent / 6N hydrochloric acid / 5 h / 25 °C View Scheme
参考文献
Ojima, Iwao; Park, Young Hoon; Sun, Chung Ming; Brigaud, Thierry; Zhao, Mangzhu
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5737 - 5740
反应条件
1: With ytterbium; methyl iodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 2 h; 2: With 1-naphthaldehyde in tetrahydrofuran T=20°C; 2 h; Further stages.;
参考文献
Jin; Makioka; Kitamura; Fujiwara
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 514 - 520
反应条件
H-Y (SiO2/Al2O3 = 5.6) zeolite T=60°C; Aza-Henry reaction; 9 h;
参考文献
Applied Catalysis A: General, , vol. 388, # 1-2 p. 211 - 215
反应条件
indium(III) chloride in acetonitrile T=20°C; Povarov type reaction; 2 h; diastereoselective reaction;
参考文献
Chemistry - A European Journal, , vol. 18, # 16 p. 5056 - 5063
反应条件
1: 96 percent / LDA / tetrahydrofuran 2: 88 percent / aq. cerium(IV) ammonium nitrate / acetonitrile 3: 98 percent / Et3N; DMAP / CH2Cl2 / 20 °C 4: 64 percent / sodium hexamethyldisilazide / tetrahydrofuran / 0.5 h / -30 °C 5: HF; pyridine / acetonitrile View Scheme
参考文献
Ojima, Iwao; Fumero-Oderda, Cecilia L.; Kuduk, Scott D.; Ma, Zhuping; Kirikae, Fumiko; Kirikae, Teruo
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 13 p. 2867 - 2888
反应条件
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran T=0°C; Inert atmosphere; 2: 4-methoxy-N-(phenylmethylene)-benzenamine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=0°C; 48 h; Inert atmosphere; 3: With hydrogenchloride; water in tetrahydrofuran T=20°C; 3 h; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 16 p. 2925 - 2928
反应条件
1: 96 percent / LDA / tetrahydrofuran 2: 88 percent / aq. cerium(IV) ammonium nitrate / acetonitrile 3: 98 percent / Et3N; DMAP / CH2Cl2 / 20 °C 4: 64 percent / sodium hexamethyldisilazide / tetrahydrofuran / 0.5 h / -30 °C 5: HF; pyridine / acetonitrile 6: 90 percent / TFA / CH2Cl2 / 0 °C View Scheme
参考文献
Ojima, Iwao; Fumero-Oderda, Cecilia L.; Kuduk, Scott D.; Ma, Zhuping; Kirikae, Fumiko; Kirikae, Teruo
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 13 p. 2867 - 2888
参考文献
Ziegler,E.; Wimmer,T.
Monatshefte fuer Chemie, 1965 , vol. 96, p. 1252 - 1260
