4-苯基-5-氨基-1,2,3-噻重氮合成路线 （共 4 条）
反应条件
hydrazine in ethanol 3 h; Heating / reflux;
参考文献
Genentech, Inc.
Patent: US2006/14700 A1, 2006 ;
Location in patent: Page/Page column 43 ;
US 20060014700 A1
反应条件
hydrazine hydrate in ethanol Heating;
参考文献
Masuda, Katsutada; Adachi, Jun; Nate, Hiroyuki; Takahata, Hidenobu; Nomura, Keiichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1591 - 1595
反应条件
1: 88 percent / toluene-p-sulphonic acid / toluene / 1.5 h / Heating 2: 92 percent / thionyl chloride / Ambient temperature 3: 79 percent / hydrazine hydrate / ethanol / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1591 - 1595
反应条件
1: 92 percent / thionyl chloride / Ambient temperature 2: 79 percent / hydrazine hydrate / ethanol / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1591 - 1595
