5-(苄氧基)-2,3-二氢-1H-茚-1-酮合成路线 （共 15 条）
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 5 - 20 °C / Inert atmosphere
1.2: 20 °C
2.1: acetonitrile / Irradiation
3.1: potassium carbonate / acetonitrile / 20 °C
View Scheme
参考文献
Sebej, Peter; Lim, Bum Hee; Park, Bong Ser; Givens, Richard S.; Klan, Petr
Organic Letters, 2011 , vol. 13, # 4 p. 644 - 647
反应条件
1.1: potassium carbonate / acetonitrile / 20 °C
2.1: copper(ll) bromide / chloroform; ethyl acetate / Reflux
3.1: sodium hydride / N,N-dimethyl-formamide / 5 - 20 °C / Inert atmosphere
3.2: 20 °C
4.1: benzene / Irradiation
View Scheme
参考文献
Sebej, Peter; Lim, Bum Hee; Park, Bong Ser; Givens, Richard S.; Klan, Petr
Organic Letters, 2011 , vol. 13, # 4 p. 644 - 647
反应条件
in benzene
Irradiation;
参考文献
Sebej, Peter; Lim, Bum Hee; Park, Bong Ser; Givens, Richard S.; Klan, Petr
Organic Letters, 2011 , vol. 13, # 4 p. 644 - 647
反应条件
hydrogenchloride; isopentyl nitrite in methanol
T=50°C; 0.5 h;
参考文献
Miyake; Itoh; Tada; Tanabe; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 7 p. 2329 - 2348
反应条件
1: potassium permanganate / benzene / |Reflux; |Dean-Stark
2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
3: acetonitrile-D3; water-d2 / |Photolysis
4: sodium tetrahydroborate / methanol-d4 / 0 °C / |Inert atmosphere
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
