1: methyl malonic acid diethylester With sodium hydride in tetrahydrofuran
T=-0.16°C; deprotonation;
2: [Pd(C4H7){o-C5H4N(CH2)2OPPh2}][O3SCF3] in tetrahydrofuran
T=18.84°C; Alkylation; 0.0166667 h; Further stages. Title compound not separated from byproducts.;
参考文献
Van Haaren, Richard J.; Druijven, Cees J. M.; Van Strijdonck, Gino P. F.; Oevering, Henk; Reek, Joost N. H.; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 10 p. 1549 - 1554
(crotyl)Pd(dppe) in tetrahydrofuran
T=18.85°C; Product distribution; Further Variations:Catalysts;
参考文献
Van Haaren, Richard J.; Van Strijdonck, Gino P. F.; Oevering, Henk; Reek, Joost N. H.; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
European Journal of Inorganic Chemistry, 2001 , # 3 p. 837 - 843
