4-羟基-5,7-二甲氧基-2-萘羧酸甲酯合成路线 （共 9 条）
反应条件
1: potassium carbonate / acetone / 16 h / Heating 2: LiAlH4 / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
sodium in methanol
0.25 h; Heating;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 610 - 627
反应条件
boron trichloride in dichloromethane
7.25 h; Ambient temperature;
参考文献
Carvalho, Christopher F.; Sargent, Melvyn V.
Journal of the Chemical Society, Chemical Communications, 1984 , # 4 p. 227 - 229
反应条件
1: 82 percent / benzene / 288 h / 20 °C
2: 63 percent / potassium acetate / 0.25 h / Heating
3: 93 percent / potassium carbonate; methanol / acetone / 3 h / 35 °C
View Scheme
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
1: 63 percent / potassium acetate / 0.25 h / Heating
2: 93 percent / potassium carbonate; methanol / acetone / 3 h / 35 °C
View Scheme
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
in solid
T=120°C; 0.1 h;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 610 - 627
反应条件
1: 92 percent / Na / methanol / 0.25 h / Heating
2: 20 percent / solid / 0.1 h / 120 °C
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 610 - 627
反应条件
potassium carbonate in acetone
16 h; Heating;
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
potassium carbonate in acetone
18 h; Heating;
参考文献
Green, Ivan R.; Hugo, Victor I.; Mei, Mawonga N.
Synthetic Communications, 2006 , vol. 36, # 3 p. 331 - 346
