2,3,4,5,6-五氟联苯合成路线 （共 79 条）
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in diethylene glycol dimethyl ether T=130°C; 24 h; Inert atmosphereSealed tube;
参考文献
Shang, Rui; Xu, Qing; Jiang, Yuan-Ye; Wang, Yan; Liu, Lei
Organic Letters, 2010 , vol. 12, # 5 p. 1000 - 1003
反应条件
silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium dichloride in dimethyl sulfoxide T=150°C; 1 h;
参考文献
Becht, Jean-Michel; Le Drian, Claude
Organic Letters, 2008 , vol. 10, # 14 p. 3161 - 3164
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in diethylene glycol dimethyl ether T=130°C; 24 h; Inert atmosphereSealed tube;
参考文献
Shang, Rui; Xu, Qing; Jiang, Yuan-Ye; Wang, Yan; Liu, Lei
Organic Letters, 2010 , vol. 12, # 5 p. 1000 - 1003
反应条件
C42H44Cl3N3Pd; potassium tert-butylate in toluene T=80°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Tu, Tao; Sun, Zheming; Fang, Weiwei; Xu, Mizhi; Zhou, Yunfei
Organic Letters, 2012 , vol. 14, # 16 p. 4250 - 4253
反应条件
1-butyl-2,2'-bipyridinium bis(trifluoromethanesulfonyl)amide; copper T=75°C; 20 h;
参考文献
Xiao, Ji-Chang; Ye, Chengfeng; Shreeve, Jean'ne M.
Organic Letters, 2005 , vol. 7, # 10 p. 1963 - 1965
反应条件
tri-tert-butyl phosphine; cesium fluoride; silver(l) oxide; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Korenaga, Toshinobu; Kosaki, Takahiro; Fukumura, Rokki; Ema, Tadashi; Sakai, Takashi
Organic Letters, 2005 , vol. 7, # 22 p. 4915 - 4917
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=80°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Ma, Xiaowei; Liu, Yan; Liu, Ping; Xie, Jianwei; Dai, Bin; Liu, Zhiyong
Applied Organometallic Chemistry, 2014 , vol. 28, # 3 p. 180 - 185
反应条件
[bmim][F] in acetonitrile T=70°C; Hiyama Coupling; 8 h; Inert atmosphere;
参考文献
Premi, Chanchal; Jain, Nidhi
European Journal of Organic Chemistry, 2013 , # 24 p. 5493 - 5499
反应条件
tris-(dibenzylideneacetone)dipalladium(0); [Pd(P{(C6H11)3})2]; lithium iodide in tetrahydrofuran T=60°C; 6 h; Inert atmosphereGlovebox; Reagent/catalystTime;
参考文献
Ohashi, Masato; Doi, Ryohei; Ogoshi, Sensuke
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 2040 - 2048
反应条件
Na3PO4*12H2O; silver carbonate; palladium dichloride in water; dimethyl sulfoxide T=100°C; 18 h; Schlenk technique; Reagent/catalystTime;
参考文献
Miao, Tao; Wang, Lei
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 429 - 436
