2,3,4,5,6-五氟联苯合成路线 （共 79 条）
反应条件
in tetrahydrofuran T=30°C; 3 h;
参考文献
Sigalov, A.B.; Petrov, E.S.; Beletskaya, I.P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 10 p. 2181 - 2183
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 10 p. 2386 - 2388
反应条件
XeF2; cesium fluoride in acetonitrile T=40°C; 1.5 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 11 p. 2580 - 2588,2297 - 2303
反应条件
XeF2; cesium fluoride in acetonitrile T=10 - 20°C; 0.333333 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 11 p. 2580 - 2588,2297 - 2303
反应条件
XeF2; cesium fluoride in acetonitrile T=10 - 20°C; 0.333333 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 11 p. 2580 - 2588,2297 - 2303
反应条件
Ag2O or CaCl(OCl) in benzene cooling;
参考文献
Journal of the Chemical Society, , p. 4966 - 4976
GB1054622 , ;
C.A., , vol. 67, p. 21597
反应条件
tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether T=20°C;
参考文献
Frohn, Hermann-Josef; Adonin, Nicolay Yu.; Bardin, Vadim V.; Starichenko, Vladimir F.
Journal of Fluorine Chemistry, 2002 , vol. 117, # 2 p. 115 - 120
反应条件
manganese triacetate Heating;
参考文献
Demir; Reis; Oezguel-Karaaslan
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 22 p. 3042 - 3045
反应条件
1: pentafluorophenyldihydroxyborane With KHF2 in methanol; water T=20°C; 4 h; 2: 4-fluoro-1-iodobenzene; dichlorobis(triphenylphosphine)palladium With silver(l) oxide in toluene T=100°C; 8 h; Further stages.;
参考文献
Tetrahedron, , vol. 64, # 25 p. 5920 - 5924
反应条件
1: pentafluorophenyldihydroxyborane With KHF2 in methanol; water T=20°C; 4 h; 2: 4-fluoro-1-iodobenzene; dichlorobis(triphenylphosphine)palladium With silver(l) oxide; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in toluene T=100°C; 8 h; Further stages.;
参考文献
Tetrahedron, , vol. 64, # 25 p. 5920 - 5924
反应条件
1: pentafluorophenyldihydroxyborane With KHF2 in methanol; water T=20°C; 4 h; 2: 4-fluoro-1-iodobenzene; dichlorobis(triphenylphosphine)palladium With silver(l) oxide; IPr*HBF4 in toluene T=100°C; 3 h; Further stages.;
参考文献
Tetrahedron, , vol. 64, # 25 p. 5920 - 5924
