2-甲基-7-甲基氨基-8-硝基-喹喔啉合成路线 （共 23 条）
反应条件
hydrogen; nickel 1.) ethanol, RT; Yield given. Multistep reaction;
参考文献
Grivas, Spiros
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 5 p. 404 - 406
反应条件
1: 1.) Fe-HCl, 2.) base View Scheme
参考文献
Kasai, Hiroshi; Shiomi, Tomoko; Sugimura, Takashi; Nishimura, Susumi
Chemistry Letters, 1981 , p. 675 - 678
反应条件
1: hydrogen / Raney nickel / ethanol / Ambient temperature
View Scheme
参考文献
Grivas, Spiros; Olsson, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1985 , vol. 39, # 1 p. 31 - 34
反应条件
1: H2 / Raney Ni / ethanol / 1 h / 760 Torr / Ambient temperature
2: 82 percent / aq. SeO2 / ethanol
3: 87 percent / conc. H2SO4, fuming HNO3 / 1 h / Ambient temperature
4: 74 percent / aq. NH4SH / methanol / 2 h / Heating
5: 11 percent / KOH / methanol; H2O / 0.17 h / Heating
6: 81 percent / 2-ethoxy-ethanol; H2O / Heating
View Scheme
参考文献
Grivas, Spiros; Tian, Wei
Acta Chemica Scandinavica, 1992 , vol. 46, # 11 p. 1109 - 1113
反应条件
in 2-ethoxy-ethanol; water
Heating;
参考文献
Grivas, Spiros; Tian, Wei
Acta Chemica Scandinavica, 1992 , vol. 46, # 11 p. 1109 - 1113
反应条件
1: 93 percent / 2-methoxy-ethanol; H2O / 0.17 h / Heating
2: 80 percent / 40percent aq. NH4SH / methanol / 3 h / Heating
3: aq. KOH / methanol / 3 h / Heating
View Scheme
参考文献
Grivas, Spiros; Tian, Wei; Ronne, Erik; Lindstroem, Stefan; Olsson, Kjell
Acta Chemica Scandinavica, 1993 , vol. 47, # 5 p. 521 - 528
反应条件
1: 80 percent / 40percent aq. NH4SH / methanol / 3 h / Heating
2: aq. KOH / methanol / 3 h / Heating
View Scheme
参考文献
Grivas, Spiros; Tian, Wei; Ronne, Erik; Lindstroem, Stefan; Olsson, Kjell
Acta Chemica Scandinavica, 1993 , vol. 47, # 5 p. 521 - 528
反应条件
1: 87 percent / conc. H2SO4, fuming HNO3 / 1 h / Ambient temperature
2: 74 percent / aq. NH4SH / methanol / 2 h / Heating
3: 11 percent / KOH / methanol; H2O / 0.17 h / Heating
4: 81 percent / 2-ethoxy-ethanol; H2O / Heating
View Scheme
参考文献
Grivas, Spiros; Tian, Wei
Acta Chemica Scandinavica, 1992 , vol. 46, # 11 p. 1109 - 1113
反应条件
1: 11 percent / KOH / methanol; H2O / 0.17 h / Heating
2: 81 percent / 2-ethoxy-ethanol; H2O / Heating
View Scheme
参考文献
Grivas, Spiros; Tian, Wei
Acta Chemica Scandinavica, 1992 , vol. 46, # 11 p. 1109 - 1113
反应条件
1: 74 percent / aq. NH4SH / methanol / 2 h / Heating
2: 11 percent / KOH / methanol; H2O / 0.17 h / Heating
3: 81 percent / 2-ethoxy-ethanol; H2O / Heating
View Scheme
参考文献
Grivas, Spiros; Tian, Wei
Acta Chemica Scandinavica, 1992 , vol. 46, # 11 p. 1109 - 1113
