5,6,7,8-四氢-gamma-氧萘-2-丁酸合成路线 （共 32 条）
反应条件
1: amalgamated zinc; hydrochloric acid
2: phosphorus pentachloride / nachfolgend Destillation im Vakuum
3: amalgamated zinc; concentrated hydrochloric acid
4: aluminium chloride / 70 - 80 °C
5: sulfur / 220 °C
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1: amalgamated zinc; hydrochloric acid
2: phosphorus pentachloride / nachfolgend Destillation im Vakuum
3: amalgamated zinc; concentrated hydrochloric acid
4: bei der Zinkstaubdestillation
5: nickel catalyst; tetralin / 120 - 150 °C / 7600 - 15200 Torr / Hydrogenation
6: nickel; tetralin / 180 °C / 10640 Torr / Hydrogenation
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Dillenschneider,J.-P.; Maire,J.-C.
Bulletin de la Societe Chimique de France, 1964 , p. 2606 - 2609
参考文献
Krollpfeiffer; Schaefer
Chemische Berichte, 1923 , vol. 56, p. 630
Show Details
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: H+, molecular sieves
2: H2 / Pd/C / acetic acid
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1: amalgamated zinc; hydrochloric acid
2: phosphorus pentachloride / nachfolgend Destillation im Vakuum
3: amalgamated zinc; concentrated hydrochloric acid
4: aluminium chloride / 70 - 80 °C
5: phosphorus pentoxide / 175 °C
6: alkali; sodium hypochlorite
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: H+, molecular sieves
3: diethyl ether
4: TosOH / benzene / Heating
5: Pd/C / Heating
View Scheme
参考文献
Chirico, R. D.; Hossenlopp, I. A.; Nguyen, A.; Steele, W. V.; Gammon, B. E.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 179 - 202
反应条件
1: amalgamated zinc; hydrochloric acid
2: phosphorus pentachloride / nachfolgend Destillation im Vakuum
3: amalgamated zinc; concentrated hydrochloric acid
4: aluminium chloride / 70 - 80 °C
5: permanganate
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: amalgamated zinc; hydrochloric acid
2: phosphorus pentachloride / nachfolgend Destillation im Vakuum
3: amalgamated zinc; concentrated hydrochloric acid
4: bei der Zinkstaubdestillation
5: nickel catalyst; tetralin / 120 - 150 °C / 7600 - 15200 Torr / Hydrogenation
6: nickel; tetralin / 180 °C / 10640 Torr / Hydrogenation
7: chromium trioxide; glacial acetic acid
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: Zn-Hg, aq. HCl / toluene / Heating
2: polyphosphoric acid / Heating
3: LiAlH4 / diethyl ether / Heating
4: KHSO4 / 150 °C
View Scheme
参考文献
Christol,H. et al.
Bulletin de la Societe Chimique de France, 1960 , p. 1576 - 1581
