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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
785-18-2
合成路线
（共 13 条）
785-18-2
→
反应条件
782-28-5
2-萘丁酸
反应条件
1: Pd-C / Heating 2: (saponification) View Scheme
参考文献
Dillenschneider,J.-P.; Maire,J.-C.
Bulletin de la Societe Chimique de France, 1964 , p. 2606 - 2609
785-18-2
→
反应条件
129-00-0
芘
反应条件
1.1: palladium 10 on activated carbon / triglyme (triethylene glycol dimethyl ether) / 4 h / 240 °C / Inert atmosphere 2.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere 3.1: n-butyllithium; N-cyclohexyl-N-isopropylamine / tetrahydrofuran; hexane / -78 °C / Inert atmosphere 3.2: 1 h / -78 °C / Inert atmosphere 4.1: palladium 10 on activated carbon / triglyme (triethylene glycol dimethyl ether) / 4 h / 240 °C / Inert atmosphere 5.1: diisobutylaluminium hydride / hexane; toluene / 1 h / -78 °C / Inert atmosphere 5.2: Inert atmosphere 6.1: methanesulfonic acid / dichloromethane / 0.5 h / 20 °C / Cooling with ice View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
785-18-2
→
反应条件
778-48-3
2,3-二氢-4(1H)-菲酮
反应条件
1: Pd-C / Heating 2: (saponification) 3: (i) SOCl2, Py, Et2O, (ii) SnCl4, benzene View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
785-17-1
5,6,7,8-四氢-gamma-氧萘-2-丁酸
→
反应条件
785-18-2
反应条件
1: H+, molecular sieves 2: H2 / Pd/C / acetic acid View Scheme
参考文献
Chirico, R. D.; Hossenlopp, I. A.; Nguyen, A.; Steele, W. V.; Gammon, B. E.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 179 - 202
119-64-2
1,2,3,4-四氢萘
→
反应条件
785-18-2
反应条件
1: AlCl3, EtNO2 2: H+, molecular sieves 3: H2 / Pd/C / acetic acid View Scheme
参考文献
Chirico, R. D.; Hossenlopp, I. A.; Nguyen, A.; Steele, W. V.; Gammon, B. E.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 179 - 202
854678-24-3
→
反应条件
785-18-2
+
782-27-4
反应条件
hydrogen; palladium on activated charcoal in acetic acid
参考文献
Chirico, R. D.; Hossenlopp, I. A.; Nguyen, A.; Steele, W. V.; Gammon, B. E.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 179 - 202
67-56-1
甲醇
→
反应条件
785-18-2
反应条件
sulfuric acid
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
529-34-0
1-四氢萘酮
→
反应条件
785-18-2
反应条件
1.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 1.2: 120 - 215 °C 2.1: AlCl3, aluminium chloride / tetrachloroethane, 1,1,2,2- / 20 °C / Cooling with ice 3.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 3.2: 120 - 215 °C 4.1: sulfuric acid / Reflux View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
1821-12-1
4-苯基丁酸
→
反应条件
785-18-2
反应条件
1.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere 2.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 2.2: 120 - 215 °C 3.1: AlCl3, aluminium chloride / tetrachloroethane, 1,1,2,2- / 20 °C / Cooling with ice 4.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 4.2: 120 - 215 °C 5.1: sulfuric acid / Reflux View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
2051-95-8
3-苯丙烯溴酸酯
→
反应条件
785-18-2
反应条件
1.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 1.2: 120 - 215 °C 2.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere 3.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 3.2: 120 - 215 °C 4.1: AlCl3, aluminium chloride / tetrachloroethane, 1,1,2,2- / 20 °C / Cooling with ice 5.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 5.2: 120 - 215 °C 6.1: sulfuric acid / Reflux View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
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