[(4-甲氧基苯基)氨基]1-氨基-9,10-二氧代蒽-2-磺酸钠合成路线 (共 2 条)
反应条件
disodium hydrogenphosphate; sodium dihydrogenphosphate; copper in water
T=100°C; Ullmann coupling reaction; P=7500.75 Torr; pH=6 - 7; 0.0833333 h; microwave irradiation;
参考文献
Baqi, Younis; Muller, Christa E.
Organic Letters, 2007 , vol. 9, # 7 p. 1271 - 1274
反应条件
sodium carbonate; copper(II) sulfate in water
T=90°C; Ullmann coupling; 48 h;
参考文献
Weyler, Stefanie; Baqi, Younis; Hillmann, Petra; Kaulich, Marko; Hunder, Andrea M.; Mueller, Ingrid A.; Mueller, Christa E.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 1 p. 223 - 227