5-甲酰基-2-甲氧基苯甲酸甲酯合成路线 （共 8 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 16 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2007/249607 A1, 2007 ;
Location in patent: Page/Page column 65; 67; 69 ;
US 20070249607 A1
反应条件
potassium carbonate in acetone 5.5 h; Heating;
参考文献
Flaherty, Daniel P.; Walsh, Shannon M.; Kiyota, Tomomi; Dong, Yuxiang; Ikezu, Tsuneya; Vennerstrom, Jonathan L.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 20 p. 4986 - 4992
反应条件
potassium carbonate in acetone T=54°C; 6 h;
参考文献
Filler, Robert; Lin, Shan; Zhang, Zhaoxu
Journal of Fluorine Chemistry, 1995 , vol. 74, p. 69 - 76
反应条件
1: 80 percent / H2SO4 / 20 h / Heating 2: 50 percent / K2CO3 / acetone / 6 h / 54 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 74, p. 69 - 76
参考文献
Journal of the Chemical Society, , vol. 121, p. 1027
反应条件
1: NaBH4 / methanol 2: SOCl2 3: n-Bu4NCl / CHCl3 View Scheme
参考文献
Miyachi, Hiroyuki; Nomura, Masahiro; Tanase, Takahiro; Takahashi, Yukie; Ide, Tomohiro; Tsunoda, Masaki; Murakami, Koji; Awano, Katsuya
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 1 p. 77 - 80
反应条件
lithium hydroxide in tetrahydrofuran; methanol; water
参考文献
Oxford GlycoSciences (UK) Ltd
Patent: US2003/216453 A1, 2003 ;
反应条件
1: NaBH4 / methanol
2: SOCl2
View Scheme
参考文献
Miyachi, Hiroyuki; Nomura, Masahiro; Tanase, Takahiro; Takahashi, Yukie; Ide, Tomohiro; Tsunoda, Masaki; Murakami, Koji; Awano, Katsuya
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 1 p. 77 - 80
