4-(反式-4-n-戊基环己基)苯乙酮合成路线 (共 16 条)
反应条件
hydrogenchloride in diethyl ether Ambient temperature;
参考文献
Liang, Jason C.; Cross, Julie O.
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 132, p. 123 - 130
反应条件
1: 2.) 10percent aq. HCl / 1.) diethyl ether, 1 h, heating 2: p-toluenesulfonic acid / toluene / Heating 3: H2 / 10percent Pd/C / ethanol 4: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: H2 / 10percent Pd/C / ethanol 2: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: H2 / 10percent Pd/C / ethanol 2: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: p-toluenesulfonic acid / toluene / Heating 2: H2 / 10percent Pd/C / ethanol 3: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: p-toluenesulfonic acid / toluene / Heating 2: H2 / 10percent Pd/C / ethanol 3: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: NaBH4 / propan-1-ol / 4 h / 30 - 35 °C 2: p-toluenesulfonic acid / toluene / Heating 3: H2 / 10percent Pd/C / ethanol 4: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
in benzene Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 114, # 4 p. 1381 - 1388
反应条件
aluminium trichloride in 1,2-dichloro-ethane 0.5 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / or in 1:1 mixture of triethanolamine and glycerol 2: AlCl3 / 1,2-dichloro-ethane / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674