4-(反式-4-n-戊基环己基)苯乙酮合成路线 （共 16 条）
反应条件
1: AlCl3 / 4 h / 45 - 50 °C 2: 80 percent NH2NH2, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating 3: AlCl3 / 3 h / 0 °C View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 88, # 1-4 p. 55 - 64
反应条件
1: 80 percent NH2NH2, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating 2: AlCl3 / 3 h / 0 °C View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 88, # 1-4 p. 55 - 64
反应条件
magnesium in tetrahydrofuran; diethyl ether 5 h; Heating; Yield given;
参考文献
Molecular crystals and liquid crystals, , vol. 116, # 1-2 p. 141 - 152
反应条件
1: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C 2: SOCl2 / 1 h / Heating 3: 69 percent / pyridine / dimethyl ether / overnight View Scheme
参考文献
Bezborodov, V. S.; Bubel', O. N.; Konovalov, V. A.; Ptashnikov, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1669 - 1674
反应条件
sodium hydroxide; bromine in 1,4-dioxane T=35 - 40°C; 3 h; Yield given;
参考文献
Szczucinski; Dabrowski
Molecular crystals and liquid crystals, 1982 , vol. 88, # 1-4 p. 55 - 64
反应条件
1: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C 2: SOCl2 / 1 h / Heating 3: 25percent aq. NH4OH 4: 62 percent / SOCl2, dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Szczucinski; Dabrowski
Molecular crystals and liquid crystals, 1982 , vol. 88, # 1-4 p. 55 - 64
