2-(3-氟-4-硝基-苯基)-丙酸乙酯合成路线 (共 2 条)
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=-45°C; 0.25 h; Inert atmosphere;
参考文献
WO2013/68463 A1, ;
Page/Page column 56 ;
反应条件
thionyl chloride 2.25 h; Cooling with ice;
参考文献
GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; SCHIENE, Klaus; DE VRY, Jean; DAMANN, Nils; LESCH, Bernhard; BAHRENBERG, Gregor; SAUNDERS, Derek John; STOCKHAUSEN, Hannelore; KIM, Yong-Soo; KIM, Myeong-Seop; LEE, Jeewoo
Patent: WO2013/68461 A1, 2013 ;
Location in patent: Page/Page column 84 ;