1: 86 percent / anhydrous potassium fluoride / 12 h / 120 - 140 °C
2: triethyl phosphite / various solvent(s) / 72 h / Heating
View Scheme
参考文献
Lindley, John M.; McRobbie, Ian M.; Meth-Cohn, Otto; Suschitzky, Hans
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 982 - 994
in ethanol
T=-173.1°C; 0.1 h; Irradiationother temperature, solvents; temperature-dependent photolysis of 1-(2-azidophenyl)-3,5-dimethylpyrazole; photolysis in glassy matrix; mechanism; formation of singlet and triplet nitrenes; thermodynamic parameters for the reactions of nitrenes; Product distribution;
参考文献
Albini, Angelo; Bettinetti, Gianfranco; Minoli, Giovanna
Journal of the American Chemical Society, 1997 , vol. 119, # 31 p. 7308 - 7315
