4'-(甲硫基)-2,2':6',2''-三联吡啶合成路线 （共 11 条）
反应条件
nickel in ethanol 6 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 47, # 16 p. 3027 - 3038
反应条件
potassium carbonate in acetonitrile
T=80 - 85°C; 2 h; Schlenk techniqueInert atmosphereMolecular sieve;
参考文献
MacHan, Charles W.; Sarjeant, Amy A.; Stern, Charlotte L.; Mirkin, Chad A.; Adelhardt, Mario; Sutter, Joerg; Meyer, Karsten
Journal of the American Chemical Society, 2012 , vol. 134, # 41 p. 16921 - 16924,4
反应条件
ammonium acetate in acetic acid
2 h; Heating;
参考文献
Potts, Kevin T.; Cipullo, Michael J.; Ralli, Philip; Theodoridis, George
Journal of Organic Chemistry, 1982 , vol. 47, # 16 p. 3027 - 3038
反应条件
1: potassium tert-butoxide / tetrahydrofuran / 14 h / Ambient temperature
2: ammonium acetate / acetic acid; tetrahydrofuran / 4 h / Heating
View Scheme
参考文献
Potts, Kevin T.; Usifer, Douglas A.; Guadalupe, Ana; Abruna, Hector D.
Journal of the American Chemical Society, 1987 , vol. 109, # 13 p. 3961 - 3967
反应条件
1: potassium tert-butoxide / tetrahydrofuran / 14 h / Ambient temperature
2: ammonium acetate / acetic acid; tetrahydrofuran / 4 h / Heating
View Scheme
参考文献
Potts, Kevin T.; Usifer, Douglas A.; Guadalupe, Ana; Abruna, Hector D.
Journal of the American Chemical Society, 1987 , vol. 109, # 13 p. 3961 - 3967
反应条件
1: sodium hydrosulfide monohydrate / N,N-dimethyl-formamide / 4 h / |Inert atmosphere; |Schlenk technique; |Reflux
2: potassium carbonate / acetonitrile / 2 h / 80 - 85 °C / |Schlenk technique; |Inert atmosphere; |Molecular sieve
View Scheme
参考文献
MacHan, Charles W.; Sarjeant, Amy A.; Stern, Charlotte L.; Mirkin, Chad A.; Adelhardt, Mario; Sutter, Joerg; Meyer, Karsten
Journal of the American Chemical Society, 2012 , vol. 134, # 41 p. 16921 - 16924,4
反应条件
ammonium acetate; potassium tert-butylate
1.) THf, room temperature, 3 h, 2.) glacial acetic acid, 2 h; Yield given. Multistep reaction;
参考文献
Potts, Kevin T.; Cipullo, Michael J.; Ralli, Philip; Theodoridis, George
Journal of the American Chemical Society, 1981 , vol. 103, # 12 p. 3585 - 3586
反应条件
Yield given. Multistep reaction;
参考文献
Cuenoud, Bernard; Schepartz, Alanna
Tetrahedron Letters, 1991 , vol. 32, # 28 p. 3325 - 3328
反应条件
NiCl2((PPh3)P)2 in diethyl ether
1.) rt, 15 min 2.) reflux, 48 h;
参考文献
Potts, Kevin T.; Usifer, Douglas A.; Guadalupe, Ana; Abruna, Hector D.
Journal of the American Chemical Society, 1987 , vol. 109, # 13 p. 3961 - 3967
参考文献
Potts, Kevin T.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 9 p. 741 - 768
