5-溴-4-肼基-6-三氟甲基嘧啶合成路线 （共 4 条）
反应条件
hydrazine hydrate in ethanol
参考文献
Ondi, Levente; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2004 , # 17 p. 3714 - 3718
反应条件
1: 86 percent / bromine; potassium acetate / acetic acid / 2 h / 80 °C
2: 77 percent / phosphorus tribromide / 0.75 h / 150 °C
3: 72 percent / hydrazine monohydrate / ethanol
View Scheme
参考文献
Ondi, Levente; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2004 , # 17 p. 3714 - 3718
反应条件
1: 70 percent / aq. hydrogen peroxide / H2O; tetrahydrofuran / 2 h / 80 °C
2: 86 percent / bromine; potassium acetate / acetic acid / 2 h / 80 °C
3: 77 percent / phosphorus tribromide / 0.75 h / 150 °C
4: 72 percent / hydrazine monohydrate / ethanol
View Scheme
参考文献
Ondi, Levente; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2004 , # 17 p. 3714 - 3718
反应条件
1: 77 percent / phosphorus tribromide / 0.75 h / 150 °C
2: 72 percent / hydrazine monohydrate / ethanol
View Scheme
参考文献
Ondi, Levente; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2004 , # 17 p. 3714 - 3718
