2,5-二氯吡啶-3-胺合成路线 （共 11 条）
反应条件
hydrogen in tetrahydrofuran; water T=120°C; P=37503.8 Torr; 15 h; chemoselective reaction;
参考文献
Jagadeesh, Rajenahally V.; Surkus, Annette-Enrica; Junge, Henrik; Pohl, Marga-Martina; Radnik, Joerg; Rabeah, Jabor; Huan, Heming; Schunemann, Volker; Brueckner, Angelika; Beller, Matthias
Science, 2013 , vol. 342, # 6162 p. 1073 - 1076
反应条件
1: phosphoryl chloride; phosphorus (V)-chloride 2: iron-turnings; acetic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 2042,2044
参考文献
Journal of the Chemical Society, , p. 2042,2044
反应条件
1: iron-turnings; acetic acid 2: aqueous HCl View Scheme
参考文献
Journal of the Chemical Society, , p. 2042,2044
反应条件
1: concentrated aqueous hydrochloric acid / -10 °C / anschliessend Behandeln mit wss. Natriumnitrit-Loesung 2: iron-turnings; acetic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 2042,2044
反应条件
potassium fluoride; hydrogen fluoride; tetrabutylammomium bromide; sodium nitrite in sulfolane; dichloromethane
参考文献
Ciba-Geigy Corporation
Patent: US4831148 A1, 1989 ;
反应条件
hydrogen fluoride; sodium nitrite in dichloromethane; dimethyl sulfoxide
参考文献
Ciba-Geigy Corporation
Patent: US4831148 A1, 1989 ;
反应条件
hydrogen fluoride; sodium nitrite in dichloromethane; water
参考文献
Ciba-Geigy Corporation
Patent: US4935051 A1, 1990 ;
反应条件
hydrogen fluoride; sodium nitrite in dichloromethane; water
参考文献
Ciba Geigy Corporation
Patent: US4713109 A1, 1987 ;
反应条件
hydrogen fluoride; sodium nitrite in dichloromethane
参考文献
Ciba-Geigy Corporation
Patent: US4831148 A1, 1989 ;
