1: MeOCH2SPh With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Metallation; 0.5 h;
2: acetone in tetrahydrofuran; hexane
T=-78°C; Condensation; 0.333333 h; Further stages.;
参考文献
Aggarwal, Varinder K.; Eames, Jason; Villa, Maria-Jesus; McIntyre, Sara; Sansbury, Francis H.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 2000 , # 4 p. 532 - 546