N-苄氧羰基-1,6-二氨基己烷盐酸盐合成路线 （共 6 条）
反应条件
1: 99 percent / NaN3 / dimethylformamide; H2O / 20 h / 80 °C 2: 60 percent / Ph3P; HCl / diethyl ether; ethyl acetate; H2O / 24 h / 20 °C 3: 100 percent / NaOH / tetrahydrofuran; H2O / 12 h / 0 - 20 °C 4: 94 percent / Ph3P / tetrahydrofuran; H2O / 24 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 14 p. 2709 - 2711
反应条件
1: 60 percent / Ph3P; HCl / diethyl ether; ethyl acetate; H2O / 24 h / 20 °C 2: 100 percent / NaOH / tetrahydrofuran; H2O / 12 h / 0 - 20 °C 3: 94 percent / Ph3P / tetrahydrofuran; H2O / 24 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 14 p. 2709 - 2711
反应条件
1: 100 percent / NaOH / tetrahydrofuran; H2O / 12 h / 0 - 20 °C 2: 94 percent / Ph3P / tetrahydrofuran; H2O / 24 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 14 p. 2709 - 2711
反应条件
hydrogenchloride 1.) methanol, 18 h; 2.) dichloromethane, 0 deg C;
参考文献
Ponpipom; Rupprecht
Carbohydrate research, 1983 , vol. 113, # 1 p. 45 - 56
反应条件
hydrogenchloride in acetic acid Yield given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 11 p. 1224 - 1227
Khimiya Geterotsiklicheskikh Soedinenii, , # 11 p. 1540 - 1544
反应条件
1: 0.1 N NaOH 2: HCl / acetic acid View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 11 p. 1224 - 1227
Khimiya Geterotsiklicheskikh Soedinenii, , # 11 p. 1540 - 1544
